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Journal Articles

Study of chemical etching conditions for alpha-particle detection and visualization using solid state nuclear track detectors

Yamada, Ryohei; Odagiri, Taiki*; Iwaoka, Kazuki*; Hosoda, Masahiro*; Tokonami, Shinji*

Radiation Environment and Medicine, 8(1), p.21 - 25, 2019/02

We evaluate radon/thoron and its progeny concentration using passive-type monitors using CR-39 plates. After exposure, it is necessary to do chemical etching for CR-39 plates. In the present study, we considered shortening of chemical etching time for CR-39 and enlargement of the track diameter (i.e. etch pit diameter) aiming for introduction of automatic counting system in the future. Optimum conditions were determined by changing solution concentration, solution temperature and etching time. As a result, the optimized conditions (concentration, temperature and etching time) were determined to be 8 M NaOH solution, 75 degrees Celsius and 10 hours. This result of etching time showed that the chemical etching was completed in less than half of conventional etching time. Furthermore, it was suggested that shorter etching time would be possible if we do not consider the enlargement of conventional track diameter.

Journal Articles

SR-excited process

Teraoka, Yuden

Nano Tekunoroji Daijiten, p.340 - 351, 2003/12

The current status of microprocesses using synchrotron radiation in Japan was reviewed. The SR-excited process is followed by SR-excited surface modification, SR-excited crystal growth and SR-excited etching. The SR-excited surface modification is followed by SR-gas-excited surface modification and SR-direct-excited surface modification. The SR-excited crystal growth is followed by SR-excited atomic layer epitaxy and SR-excited chemical vapor deposition. THe SR-excited etching is followed by SR-direct-excited etching, SR-gas-excited etching and SR ablation.

Journal Articles

Observation of nuclear track development in polyvinylidene fluoride with several etchants

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J.Electron Microsc., 30(4), p.292 - 297, 1981/00

no abstracts in English

Journal Articles

Growth of fine holes by the chemical etching of fission tracks in polyvinylidene fluoride

Nucl.Tracks, 13(1-2), p.33 - 44, 1979/00

no abstracts in English

Journal Articles

Chemical etching of fission tracks in polyfluoro plastic

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Science, 199(4327), p.421 - 422, 1978/00

 Times Cited Count:14

no abstracts in English

Journal Articles

Growth of fine holes in polyethylenenaphthalate film irradiated by fission fragments

;

Journal of Applied Physics, 47(4), p.1355 - 1358, 1976/04

 Times Cited Count:13

no abstracts in English

Journal Articles

Electron microscopy of fine holes in polyethyleneterephthalate films irradiated by fission fragments

; ; Izui, Kazuhiko;

Journal of Applied Physics, 46(3), p.1155 - 1158, 1975/03

 Times Cited Count:6

no abstracts in English

Journal Articles

Identification of Dislocations in NaF Crystals by Electrolytic Coloration and Chemical Etching

Journal of the Physical Society of Japan, 26(1), p.143 - 148, 1969/01

 Times Cited Count:5

no abstracts in English

Journal Articles

Identification of dislocation in NaF crystals by electrolytic coloration and chemical etching

Journal of the Physical Society of Japan, 26(1), p.143 - 148, 1969/00

no abstracts in English

Oral presentation

Preparation of metal nano-needles using ion-track membranes

Koshikawa, Hiroshi; Yamamoto, Shunya; Sugimoto, Masaki; Kitamura, Akane; Sawada, Shinichi; Yamaki, Tetsuya

no journal, , 

Chemical etching of polymer films irradiated with heavy ions leads to the formation of ion-track membranes with nanoscale pores in different shapes. Particularly, conically-shaped pores are expected to have a potential to create metallic nanoneedles by combination of vapor-deposition and electroplating methods. In this study, we prepared copper nanoneedles inside the conical pores of polyimide (PI)-based ion-track membranes and investigated their morphology. The PI films were irradiated with $$^{40}$$Ar ions. The irradiated films were etched in a sodium hypochlorite solution at 60$$^{circ}$$C for 0.5 h, leading to the formation of conical pores with a surface diameter of ca. 500 nm. A very thin Au layer was deposited on this pore side of the ion-track membranes; then, it was used as a cathode for electroplating copper into the pores. After dissolving the PI templates, we obtained the copper needles ca. 500 nm in base diameter and 1.2 $$mu$$m in height on copper plates.

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